HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl chloroformate → HCID 58288710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | 5-tert-Butyl-3-methylpyrocatechol | HCID 75173 | — |
| Product | HCID 58288710 | HCID 58288710 | 75.2% |
Reaction Steps
Prepared from 5-tert-butyl-3-methylbenzene-1,2-diol and phenyl chloroformate; purified by recrystallization from ethanol to yield a while solid (75.2%); 1H NMR (500 MHz, CDCl3, ppm): δ 7.35-7.38 (m, 4H), 7.23-7.28 (m, 7H), 7.16-7.17 (m, 1H), 2.36 (s, 3H), 1.32 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263520B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-0452d21693b3499889a21b45a4ca42dc |
| Source note | uspto-grants-2012_09 |