HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68725603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68725929 | HCID 68725929 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68725603 | HCID 68725603 | — |
Reaction Steps
4M HCl in dioxane (1.2 ml) is added to a stirred solution of {4-[5-(2-amino-4-methyl-pyrimidin-5-yl)-2-chloro-benzenesulfonylamino]-cyclohexylmethyl}-carbamic acid tert-butyl ester (Example 3-17) (0.25 g, 0.49 mmol) in dioxane (1 ml). After 18 h the solvent is removed to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263585B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-ef2e9dc8066048518518c2cb1c4d849d |
| Source note | uspto-grants-2012_09 |