HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58748417, compound → HCID 58748479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58748417 | HCID 58748417 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58748479 | HCID 58748479 | — |
Reaction Steps
A suspension of 4′-methoxy-4-methyl-3-nitrobiphenyl (630 mg, 2.95 mmol) and 10% palladium on charcoal (63 mg, 0.059 mmol) in methanol (6 mL) is stirred under hydrogen atmosphere for 12 hours. Palladium catalyst is removed by filtration and the resulting solution is evaporated in vacuo to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263590B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-770ce03128dd47f59d11f268093dbb84 |
| Source note | uspto-grants-2012_09 |