HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-(6-bromo[1,2,4]triazolo[1,5-a]pyridin-2-yl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 6-Bromo-[1,2,4]triazolo[1,5-a]pyridin-2-amine | HCID 25215940 | — |
| Product | N-(6-bromo[1,2,4]triazolo[1,5-a]pyridin-2-yl)benzamide | HCID 25212517 | — |
Reaction Steps
The title compound was prepared following procedure described for intermediate B1, but starting from 6-bromo[1,2,4]triazolo[1,5-a]pyridin-2-amine ((AS), 5.0 g; 23.47 mmol; 1.0 eq.) and benzoyl chloride (6.57 g; 46.9 mmol; 2.0 eq.) as a white powder (6.5 g, 87%). HPLC, Rt: 2.49 min. (purity 97.1%). LC/MS, M+(ESI): 317.0, M−(ESI): 316.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263595B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-b034ae7efb1c4c648f6a5e0a54062eab |
| Source note | uspto-grants-2012_09 |