HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 59437435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | N-(5-bromo[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide | HCID 25212514 | — |
| Product | HCID 59437435 | HCID 59437435 | — |
Reaction Steps
The title compound was prepared following procedure and work up described for example 30, but starting from N-(5-bromo[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide ((B2), 50 mg; 0.16 mmol; 1.0 eq.) and pyrrolidine (1 mL) as a white solid (1 mg, 2%). HPLC, Rt: 1.81 min. (purity 97.3%). LC/MS, M+(ESI): 309.4, M−(ESI): 307.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263595B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-82b1014aeff94b8a8f9d2e4bc01b54d4 |
| Source note | uspto-grants-2012_09 |