HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Butylbenzoic acid → 4-butyl-N-[5-(3-furyl)[1,2,4]triazolo[1,5-a]pyridin-2-yl]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Butylbenzoic acid | HCID 88631 | — |
| Reactant | 5-(Furan-3-yl)-[1,2,4]triazolo[1,5-a]pyridin-2-amine | HCID 25215938 | — |
| Product | 4-butyl-N-[5-(3-furyl)[1,2,4]triazolo[1,5-a]pyridin-2-yl]benzamide | HCID 25213977 | — |
Reaction Steps
The title compound was prepared following procedure and work up described for example 2, but starting from 5-(3-furyl)[1,2,4]triazolo[1,5-a]pyridin-2-amine ((A2), 75 mg; 0.37 mmol; 1.0 eq.) and 4-butylbenzoic acid (80 mg; 0.45 mmol; 1.2 eq.) as a yellow foam (20 mg, 15%). HPLC, Rt: 4.45 min. (purity 82.6%). LC/MS, M+(ESI): 361.1, M−(ESI): 359.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263595B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-89aa92c447cf425aaa9a9cf734ea9a19 |
| Source note | uspto-grants-2012_09 |