HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylcyclohexylamine → HCID 25214210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylcyclohexylamine | HCID 7514 | — |
| Reactant | N-(5-chloro[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide | HCID 25212516 | — |
| Product | HCID 25214210 | HCID 25214210 | — |
Reaction Steps
The title compound was prepared following procedure described for example 30 but starting from N-(5-chloro[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide ((B4), 55 mg; 0.20 mmol; 1.0 eq.) and N-methylcyclohexylamine (1.0 mL) as an off white solid (30 mg, 43%). HPLC, Rt: 2.67 min. (purity 97.8%). LC/MS, M+(ESI): 351.4, M−(ESI): 349.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263595B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-159ca27e60fc4dda9f9c5193baaec60e |
| Source note | uspto-grants-2012_09 |