HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67309189, compound → HCID 15539217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67309189 | HCID 67309189 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15539217 | HCID 15539217 | 98.9% |
Reaction Steps
To a solution of 8-bromo-4-hydroxy-7-methylnaphthalene-2-carboxylic acid (0.45 g) in ethanol (8 mL) was added palladium-carbon (180 mg) in 3 parts, and the mixture was stirred at room temperature for 2 days under a hydrogen atmosphere. The insoluble material was removed by filtering through a Celite pad, and the filtrate was concentrated to give the title compound (0.32 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263622B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-8a76776f05be4de3989f4d05de0a35ab |
| Source note | uspto-grants-2012_09 |