HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86684861, compound → HCID 86684860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86684861 | HCID 86684861 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86684860 | HCID 86684860 | 104.3% |
Reaction Steps
10% palladium carbon (20 mg) was added to an ethanol (2.4 mL) solution of 5-[4-(cyclopenta-1-ene-1-yl)phenyl]-1-methyl-1H-pyrazole (133 mg), and the obtained solution was then stirred under a hydrogen atmosphere at a room temperature overnight. Thereafter, the reaction solution was filtrated with Celite, and the filtrate was then concentrated under a reduced pressure, so as to obtain the title compound (140 mg) in the form of a light yellow oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642626B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-c4ea02a7f6f640d98431336921bedb3d |
| Source note | uspto-grants-2014_02 |