HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58297375, compound → HCID 58297373, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58297375 | HCID 58297375 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 58297373 | HCID 58297373 | 118.3% |
Reaction Steps
A solution of tert-butyl 2-(2-(4-cyano-2-methylphenyl)-3-(4-methoxyphenyl)-1H-pyrrol-1-yl)ethylcarbamate (6-1) (110 mg, 0.255 mmol) in methanolic hydrochloride solution (2 M, 5 mL) was stirred at room temperature for 1 hour. The mixture was concentrated in vacuo to give the title compound 6-2 (100 mg), which was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642628B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-ff93f1ec12d74732a41dab33ae24f918 |
| Source note | uspto-grants-2014_02 |