HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorosalicylic Acid → 2-(5-Chloro-2-hydroxybenzoyl)amino-4,5,6,7-tetrahydrobenzo[b]-thiophene-3-carboxylic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorosalicylic Acid | HCID 9447 | — |
| Reactant | Ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate | HCID 78262 | — |
| Product | 2-(5-Chloro-2-hydroxybenzoyl)amino-4,5,6,7-tetrahydrobenzo[b]-thiophene-3-carboxylic acid ethyl ester | HCID 10068311 | 49.6% |
Reaction Steps
Using 5-chlorosalicylic acid and 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylic acid ethyl ester as the raw materials, the same operation as the example 16 gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263657B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-5bf4280aab9d403c85c5b570049a2b6b |
| Source note | uspto-grants-2012_09 |