5-Nitrosalicylic acid → HCID 17860147, compound

HRID 2384439Notes

Reaction equation

HRID 2384439 reaction equation
[N+:1]([C:4]1[CH:12]=[C:8]([C:9]([OH:11])=O)[C:7]([OH:13])=[CH:6][CH:5]=1)([O-:3])=[O:2].[Cl:14][C:15]1[CH:16]=[C:17]([CH:19]=[C:20]([Cl:22])[CH:21]=1)[NH2:18]>>[Cl:14][C:15]1[CH:16]=[C:17]([NH:18][C:9](=[O:11])[C:8]2[CH:12]=[C:4]([N+:1]([O-:3])=[O:2])[CH:5]=[CH:6][C:7]=2[OH:13])[CH:19]=[C:20]([Cl:22])[CH:21]=1

Participants

3

Reactant 2

HCID 73185-Nitrosalicylic acidHCID 122813,5-Dichloroaniline

Product 1

HCID 17860147HCID 17860147, compoundYield 83.1%

Procedure

Using 5-nitrosalicylic acid and 3,5-dichloroaniline as the raw materials, the same operation as the example 16 gave the title compound.

Sources & evidence

ORD record
ord-a9849f3ac25642b5999cc9be96adac79
Source dataset
uspto-grants-2012_09
Patent number
US08263657B2

Reaction notes

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