反应详情

温度

85 °C

A mixture of 5.9 gm of 2-chloro-4,6-bis(4-phenoxyphenyl)-1,3,5-triazine, 2.6 gm aluminum chloride and 1.6 gm of resorcinol in 25 ml chlorobenzene was heated under nitrogen at 85° C. for 3 hr. An additional 0.17 gm resorcinol was added, and the heating continued for another 1 hr. The reaction mixture was cooled to room temperature, and quenched with water. The precipitated product was filtered, washed with water, and dried to give 5.1 gm of crude 2-(2,4-dihydroxyphenyl)-4,6-bis(4-phenoxyphenyl)-1,3,5-triazine.

1. temperatureThe reaction mixture was cooled to room temperature
2. customquenched with water
3. filtrationThe precipitated product was filtered
4. washwashed with water
5. customdried