HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 24803739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 24803740 | HCID 24803740 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 24803739 | HCID 24803739 | 79% |
Reaction Steps
Prepare the HCl salt by dissolving the free base in dichloromethane and MeOH. Treat the mixture with 1.0 M HCl in EtOH, add Et2O, filter, and wash with Et2O. Dry in a vacuum oven at RT for 2 days to give 0.249 g (79%) of the title compound. LC-MS/ES m/z (35Cl) 480.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263772B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-319f7292d75e47319eb1f815a299277c |
| Source note | uspto-grants-2012_09 |