HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57828142, compound → HCID 57828147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57828142 | HCID 57828142 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 57828147 | HCID 57828147 | — |
Reaction Steps
8 g (0.0170 mol) of (12-benzyloxy-6,9-bis(carboxymethyl)-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(14),11(15),12-trien-3-yl)acetic acid are added to 100 ml of 10N HCl. The mixture is left to react overnight at 40° C. It is concentrated. The product is crystallized from acetone. w=6 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268810B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-d0c912e73ceb4778886828ed54a8555b |
| Source note | uspto-grants-2012_09 |