Oleylamine → Octadecylamine

HRID 2386211Notes

Reaction equation

HRID 2386211 reaction equation
[CH2:1]([NH2:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[H][H]>C(O)C.[Pd]>[CH2:1]([NH2:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

5

Reactant 2

HCID 5356789OleylamineHCID 178418361HCID 178418361, compound

Product 1

HCID 15793Octadecylamine

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

2 g of oleylamine in 120 ml of ethanol are hydrogenated at 30° C. under 8 bar of hydrogen in the presence of palladium-on-charcoal. After reacting for 4 h and evaporating the solvent, 1.6 g of product are obtained in the form of a white powder.

Workup

  1. customevaporating the solvent, 1.6 g of product
  2. customare obtained in the form of a white powder

Sources & evidence

ORD record
ord-db47587655114fdb9576b31622f2b5c0
Source dataset
uspto-grants-2012_09
Patent number
US08268810B2

Reaction notes

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