HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-benzyl-3-methylmorpholine-3-carboxylate → Methyl 3-methylmorpholine-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-benzyl-3-methylmorpholine-3-carboxylate | HCID 67268304 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Methyl 3-methylmorpholine-3-carboxylate | HCID 67268303 | — |
Reaction Steps
Dissolve methyl 4-benzyl-3-methylmorpholine-3-carboxylate in EtOH (10 volumes) and add 10% Pd/C (0.1 eq.). Hydrogenate for 16 hours, filter through Celite®, and concentrate to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268819B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-6d34390c0fae4263937b91c0e0f08259 |
| Source note | uspto-grants-2012_09 |