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HRID2386383

反应详情

EQUATION

反应方程式

HRID 2386383 的结构方程式

REACTANTS

反应物

2
结构：NCCc1ccc(O)cc1
HCID5610

Tyramine

C8H11NO

结构：COC(OC)c1cccc(-c2ccnc(Cl)n2)c1
HCID86603261

未命名化合物

PRODUCTS

生成物

1
结构：COC(OC)c1cccc(-c2ccnc(NCCc3ccc(O)cc3)n2)c1
HCID67045057

未命名化合物

收率 35%

PROCEDURE

实验过程

Intermediate 26 was coupled with tyramine following procedure F. The product was purified by flash chromatography using 99:1 CH2Cl2:MeOH as eluent. Yield: 35%. LC-MS showed the product had the expected M+H+ of 366.

WORKUP

后处理

  1. customThe product was purified by flash chromatography