HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → 4-(2-propen-1-yl)-2H-1,4-Benzoxazin-3(4H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 2H-1,4-benzoxazin-3(4H)-one | HCID 72757 | — |
| Product | 4-(2-propen-1-yl)-2H-1,4-Benzoxazin-3(4H)-one | HCID 57346023 | — |
Reaction Steps
In analogy to Example 64, step 1, 2H-1,4-benzoxazin-3(4H)-one (15 g) was reacted with 3-bromo-propene to give the title compound (17.4 g) as a colorless oil. MS (m/e)=190.3 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268820B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-72aef05e118a45f7a908fef675a602cf |
| Source note | uspto-grants-2012_09 |