HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4-nitrophenol → 4-Amino-2-bromophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4-nitrophenol | HCID 22109 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Amino-2-bromophenol | HCID 14440265 | — |
Reaction Steps
The target compound was obtained by reducing 2-bromo-4-nitrophenol with iron in a mixed solution of methanol and ammonium chloride aqueous solution. 2-bromo-4-nitrophenol was manufactured by the method described in the literature (J. Org. Chem., Vol. 62, 1997, p. 4504).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268842B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-5a4a848ad6ad4a9bb141bd1e26fb4728 |
| Source note | uspto-grants-2012_09 |