Sodium Acetate → HCID 68500140, compound

Participants

Reaction Steps

To a solution of intermediate B2 in acetic acid (0.16 M) was added NaOAc (2 eq.) and the mixture was stirred and heated to reflux for 1 h. The solution was cooled to RT and the solvent was removed under reduced pressure. The residue was suspended in water and triturated until a fine suspension was obtained. The solid material was filtered off, washed with water, dried by air stream and then under high vacuum. MS (ES) C14H12FN3O required: 257, found: 258 (M+H)+.

Provenance & Evidence