HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68505044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86761616 | HCID 86761616 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68505044 | HCID 68505044 | — |
Reaction Steps
Crude II2 was dissolved in EtOAc, then 4M HCl in dioxane was added. The mixture was stirred at RT for 30 min. After the removal of the solvent under reduced pressure, the crude was scratched with Et2O and the solvent decanted to afford the title compound (II3). MS (ES) C9H17ClN2O2 requires: 184, found: 185 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268827B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-a56ff2b2e1ff4305961edd781df821e1 |
| Source note | uspto-grants-2012_09 |