HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methylpyridine-2-carbonitrile → HCID 68501679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methylpyridine-2-carbonitrile | HCID 74182 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 68501679 | HCID 68501679 | — |
Reaction Steps
To a solution (4.0 M) of 6-methyl-2-pyridinecarbonitrile in TFA was added PtO2 (0.1 eq) and the mixture was stirred for 50 h under H2 atmosphere at 50 psi. The reaction mixture was filtered and concentrated at reduced pressure to afford the title compound SS1. MS (ES) C7H16N2 required: 128, found: 129 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268827B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-27dec233dff445a2bedd07710d93462e |
| Source note | uspto-grants-2012_09 |