Hydrochloric Acid → HCID 18440640, compound

Participants

Reaction Conditions

Reaction Steps

2-Amino-benzamide (1 g, 7.3 mmol) was dissolved in chloroform (25 ml) in a 50 ml round bottomed flask and cooled to 0° C. Pyridine (0.6 ml, 7.3 mmol) was added followed by 2-fluoro-benzoyl chloride (1 ml, 8 mmol) and the mixture was magnetically stirred for 1 hr at this temperature. 10% Hydrochloric acid (50 ml) was added and the precipitated solid was filtered, washed with water and dried to yield pure title compound (1.56 g, 82%).

Provenance & Evidence