HRID2387750

反应详情

EQUATION

反应方程式

HRID 2387750 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The compound 326-4 (1.42 g) was dissolved in ethyl acetate (30 ml). Palladium-carbon (700 mg) was added to the solution, and the obtained mixture was stirred in a hydrogen atmosphere for 1 hour. The reaction mixture was filtered with Celite, and the filtrate was concentrated under reduced pressure, so as to obtain the crude title compound (954 mg).

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered with Celite
  2. concentrationthe filtrate was concentrated under reduced pressure