HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentylamine → HCID 68415787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentylamine | HCID 8060 | — |
| Reactant | 2-Amino-4-chloro-6-methylpyrimidine | HCID 21810 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68415787 | HCID 68415787 | — |
Reaction Steps
2-Amino-4-chloro-6-methylpyrimidine (10 g) and pentylamine (20 ml) were combined in dioxane (100 mL) and refluxed for 42 h. The solvents were evaporated, the product taken up in DCM, washed with water, sat. sodium bicarbonate solution, brine, dried, and the solvent evaporated to give the subtitle compound 8.3 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268990B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-190a6037f4744643a691018ca798b579 |
| Source note | uspto-grants-2012_09 |