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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2387772Generated: October 31, 2026

Pentylamine → HCID 68415787, compound

https://huagongshe.com/reaction/2387772

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPentylamineHCID 8060—
Reactant2-Amino-4-chloro-6-methylpyrimidineHCID 21810—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 68415787HCID 68415787—

Reaction Steps

2-Amino-4-chloro-6-methylpyrimidine (10 g) and pentylamine (20 ml) were combined in dioxane (100 mL) and refluxed for 42 h. The solvents were evaporated, the product taken up in DCM, washed with water, sat. sodium bicarbonate solution, brine, dried, and the solvent evaporated to give the subtitle compound 8.3 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08268990B2
Source datasetuspto-grants-2012_09
ORD IDord-190a6037f4744643a691018ca798b579
Source noteuspto-grants-2012_09