HRID2387779

反应详情

EQUATION

反应方程式

HRID 2387779 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The product from step (i) (0.1 g) was dissolved in MeOH and dimethylamine (2M in MeOH, 0.61 ml) was added. The reaction mixture was stirred for 72 h at rt, the solvents were evaporated and the residue purified by RPHPLC to give the title compound 24 mg.

WORKUP

后处理

  1. customthe solvents were evaporated
  2. customthe residue purified by RPHPLC