HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178433372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Guanidine | HCID 3520 | — |
| Reactant | Methyl 2-(4-(cyanomethyl)benzyl)-3-oxobutanoate | HCID 59590640 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178433372 | HCID 178433372 | — |
Reaction Steps
A mixture of the crude product from step (i) and guanidine (16 g) in EtOH (350 ml) was heated under reflux for 5 h. The mixture was cooled, neutralised with acetic acid, and the solid filtered and dried, 22.1 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268990B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-5b16fe2b445c4de69d59080041956064 |
| Source note | uspto-grants-2012_09 |