Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pentylamine | HCID 8060 | — |
| Reactant | HCID 86633416 | HCID 86633416 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 68955280 | HCID 68955280 | — |
Reaction Steps
The product from step (iii) (Ig) was combined with butan-1-ol (25 mL) and pentan-1-amine (4 mL) was added. The reaction mixture was heated to 110° C. for 18 h. The solvents were evaporated and the product purified using chromatography to give the subtitle compound as an orange oil, 600 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08268990B2 |
|---|
| Source dataset | uspto-grants-2012_09 |
|---|
| ORD ID | ord-6a9f034aa561408bae7b427948650613 |
|---|
| Source note | uspto-grants-2012_09 |
|---|
