HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178433377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178433379 | HCID 178433379 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178433377 | HCID 178433377 | — |
Reaction Steps
SOCl2 (20 ml) was added slowly to a stirred mixture of the product from step (i) (6.7 g) in DCM (50 ml) and stirred at rt for 24 h. The solvent was evaporated under reduced pressure to give the title compound, 8.7 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268990B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-375d893d8c2847f3b479921493a68464 |
| Source note | uspto-grants-2012_09 |