Iodoethane → HCID 59541826, compound

HRID 2388326Notes

Reaction equation

HRID 2388326 reaction equation
[O:1]1[C:5]2([CH2:10][CH2:9][C:8]([C:11]3[CH:12]=[CH:13][C:14](=[O:17])[NH:15][CH:16]=3)=[CH:7][CH2:6]2)[O:4][CH2:3][CH2:2]1.[CH2:18](I)[CH3:19]>>[O:4]1[C:5]2([CH2:10][CH2:9][CH:8]([C:11]3[CH:12]=[CH:13][C:14](=[O:17])[N:15]([CH2:18][CH3:19])[CH:16]=3)[CH2:7][CH2:6]2)[O:1][CH2:2][CH2:3]1

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 66750331HCID 66750331, compound

Product 1

HCID 59541826HCID 59541826, compound

Procedure

The title compound was prepared as a white solid from the ethylation of 5-(1,4-dioxa-spiro[4.5]dec-7-en-8-yl)-1H-pyridin-2-one with EtI (Aldrich) using the procedure described in Step B of Example 38.

Sources & evidence

ORD record
ord-e8087d71f7de42349acf72e0dc9c8927
Source dataset
uspto-grants-2012_09
Patent number
US08269015B2

Reaction notes

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