HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 66750436, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 4-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)pyridine | HCID 13772054 | — |
| Product | HCID 66750436 | HCID 66750436 | — |
Reaction Steps
4-(1,4-Dioxa-spiro[4.5]dec-7-en-8-yl)-pyridine (as prepared in the previous step, 1.5 g, 6.91 mmol) in MeI (˜10 mL) was heated to reflux until the precipitate was completely dissolved. The reaction was cooled and filtered to collect the brown solid as the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08269015B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-41bcb0a6e77b4ac2a44f5aaf1c81b085 |
| Source note | uspto-grants-2012_09 |