HRID2388356
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
{1-[4-(5-Trichloromethyl-[1,2,4]oxadiazol-3-yl)-cyclohexyl]-azetidin-3-yl}-carbamic acid tert-butyl ester (as prepared in the previous step) was treated with 1:1 ratio of DCM and TFA at room temperature. After 2 hours, the solvent was removed in vacuo and the residue was dried overnight to give the title compound as TFA salt (colorless oil).
WORKUP
后处理
- customthe solvent was removed in vacuo
- customthe residue was dried overnight