Hydrochloric Acid → HCID 59541821, compound

Participants

Reaction Steps

A solution of 2-(1,4-dioxa-spiro[4.5]dec-8-yl)-5,6,7,8-tetrahydro-[1,2,4]triazolo[1,5-a]pyridine (1.05 g, 4 mmol, prepared according to the literature procedure: Quanrui Wang, Atef Amer, Susanne Mohr, Eveline Ertel, Johannes C. Jochims, Tetrahedron, 1993, 49(44), 9973-9986) in CH3CN (20 mL) and 2N HCl (30 mL) was stirred at rt for 2 h. Evaporation to dryness gave the intermediate as a HCl salt.

Provenance & Evidence