HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 68644004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | HCID 68644058 | HCID 68644058 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 68644004 | HCID 68644004 | — |
Reaction Steps
5-tert-Butyl 3-ethyl 4-phenyl-6,7-dihydroisoxazolo[4,5-c]pyridine-3,5(4H)-dicarboxylate (1.75 mmol) was hydrolyzed to corresponding acid by using LiOH.H2O (1.5 eq.) as a base in ethanol-water (10 ml, 4:1). Yield: quantitative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268814B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-cbb239964d9c4d93b7fcf107c40aa365 |
| Source note | uspto-grants-2012_09 |