HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → N-(4-chloro-3-(quinoxalin-3-yl)phenyl)-3,5-dimethoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | N-(3-(2-bromoacetyl)-4-chlorophenyl)-3,5-dimethoxybenzamide | HCID 86623924 | — |
| Product | N-(4-chloro-3-(quinoxalin-3-yl)phenyl)-3,5-dimethoxybenzamide | HCID 11589824 | — |
Reaction Steps
Procedure D was performed using N-(3-(2-bromoacetyl)-4-chlorophenyl)-3,5-dimethoxybenzamide (0.029 g, 0.07 mmol), 1,2-phenylenediamine (0.021 g, 0.19 mmol) and DIPEA (0.042 ml, 0.24 mmol) to give N-(4-chloro-3-(quinoxalin-3-yl)phenyl)-3,5-dimethoxybenzamide as a light tan powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273743B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-17c8bca2ef8b46dfaf491f12e37d8883 |
| Source note | uspto-grants-2012_09 |