HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → 5-(4-bromophenyl)-1H-indole-3-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 59145397 | HCID 59145397 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-(4-bromophenyl)-1H-indole-3-carboxamide | HCID 59145417 | — |
Reaction Steps
A solution of 4 (1.00 g, 3.38 mmol) in ethanol was treated with hydrogen peroxide (30%) and 1N NaOH. On completion of reaction solvent was removed and the resultant solid was washed with organic solvents to give pure 5 as a beige colored solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273744B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-28903cc526434bc8b434ac5b5234469d |
| Source note | uspto-grants-2012_09 |