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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2389348Generated: October 30, 2026

HCID 86637908, compound → HCID 68540248, compound

https://huagongshe.com/reaction/2389348

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86637908HCID 86637908—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 68540248HCID 6854024890.9%

Reaction Steps

To a solution of methyl (2E)-3-[3-(3-hydroxypropyl)phenoxy]acrylate (300 mg) in MeOH (4.0 mL) was added 10% palladium on carbon (50 mg) at ambient temperature and the mixture was stirred at ambient temperature for 4 hours under hydrogen atmosphere (3 atms). The mixture was filtered through a bed of celite. The filtrate was evaporated in vacuo to afford methyl 3-[3-(3-hydroxypropyl)phenoxy]propanoate (275 mg) as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273745B2
Source datasetuspto-grants-2012_09
ORD IDord-263123cf9c3443868e6af5f197de7d6f
Source noteuspto-grants-2012_09