HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86637908, compound → HCID 68540248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86637908 | HCID 86637908 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68540248 | HCID 68540248 | 90.9% |
Reaction Steps
To a solution of methyl (2E)-3-[3-(3-hydroxypropyl)phenoxy]acrylate (300 mg) in MeOH (4.0 mL) was added 10% palladium on carbon (50 mg) at ambient temperature and the mixture was stirred at ambient temperature for 4 hours under hydrogen atmosphere (3 atms). The mixture was filtered through a bed of celite. The filtrate was evaporated in vacuo to afford methyl 3-[3-(3-hydroxypropyl)phenoxy]propanoate (275 mg) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273745B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-263123cf9c3443868e6af5f197de7d6f |
| Source note | uspto-grants-2012_09 |