HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 86637911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 86637913 | HCID 86637913 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86637911 | HCID 86637911 | — |
Reaction Steps
To a solution of ethyl (4-{3-[(tert-butoxycarbonyl)amino]propyl}phenoxy)acetate (2.5 g) in EtOAc (7.5 mL) was added 4 M HCl/EtOAc (10 mL) at ambient temperature. After stirring for 5 hours at ambient temperature, the mixture was evaporated in vacuo to give a ethyl [4-(3-aminopropyl)phenoxy]acetate hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273745B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-7c9af6565a4243e8838718e8daaf8d8e |
| Source note | uspto-grants-2012_09 |