HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59400108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | tert-butyl 1-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-4-ylcarbamate | HCID 59400071 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59400108 | HCID 59400108 | — |
Reaction Steps
To a solution of 1 tert-butyl 1-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-4-ylcarbamate in dichloromethane (2 mL) was added HCl (4 M in 1,4-dioxane, 2 mL, 8.0 mmol). The mixture was stirred at room temperature for 20 hours before being filtered and evaporated to dryness to yield 1-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-4-amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273754B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-17a00cab29c645b897368826039692cf |
| Source note | uspto-grants-2012_09 |