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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2389647Generated: October 31, 2026

Methylamine → HCID 59683621, compound

https://huagongshe.com/reaction/2389647

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethylamineHCID 6329—
ReactantHCID 59683538HCID 59683538—
SolventMethanolHCID 887—
ProductHCID 59683621HCID 59683621—

Reaction Steps

A stirred solution of methyl ester 148 (30 mg, 0.05 mmol) in MeOH (2 mL) is treated with methylamine (1 mL, 40% solution in water) at RT. After 1 h, the reaction mixture is reduced in vacuo and the residue purified by column chromatography (75% EtOAc in heptane) to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273747B2
Source datasetuspto-grants-2012_09
ORD IDord-d238887dec564d53a70c5d9fffa618e0
Source noteuspto-grants-2012_09