HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 59683621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 59683538 | HCID 59683538 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59683621 | HCID 59683621 | — |
Reaction Steps
A stirred solution of methyl ester 148 (30 mg, 0.05 mmol) in MeOH (2 mL) is treated with methylamine (1 mL, 40% solution in water) at RT. After 1 h, the reaction mixture is reduced in vacuo and the residue purified by column chromatography (75% EtOAc in heptane) to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273747B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-d238887dec564d53a70c5d9fffa618e0 |
| Source note | uspto-grants-2012_09 |