Hexane → HCID 86618978, compound

Participants

Reaction Steps

tert-Butyl carbamate 205 (23 mg, 31 mmol) is deprotected using Method F. The isolated salt is then dissolved in the minimum amount of DCM and added dropwise to cold (0° C.) hexane (10 mL). The resultant cream precipitate is isolated by filtration and dried to afford the title compound.

Provenance & Evidence