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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2389716Generated: November 1, 2026

HCID 178454052, compound → HCID 178418966, compound

https://huagongshe.com/reaction/2389716

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178454052HCID 178454052—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 178418966HCID 178418966—

Reaction Steps

Cbz BOC diamine (294) (458 mg, 1.05 mmol) (containing residual benzyl alcohol) and 10% palladium on charcoal (92 mg, 20% by weight) in EtOH (9 mL) was stirred under a hydrogen atmosphere until the reaction was complete. The reaction was filtered through celite, washed with more EtOH and reduced in vacuo to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273747B2
Source datasetuspto-grants-2012_09
ORD IDord-a0905112f8cd4a8fb1de498eb929cd9b
Source noteuspto-grants-2012_09