HCID 68950348, compound → HCID 86636899, compound

Participants

Reaction Steps

tert-Butyl 3-(4-(5-chloro-N,3-dimethylbenzo[b]thiophene-2-sulfonamido)phenyl)azetidine-1-carboxylate (185 mg, 0.36 mmol) was stirred in formic acid (3 ml) at 0° C. for 3.5 h. The solution was concentrated, dissolved in water, concentrated HCl was added and the solution was concentrated by lyophylisation to give the title compound (144 mg, 87%) as a white foam.

Provenance & Evidence