HRID2389885
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Furo[3,2-c]pyrazolo[1,5-a]pyridin-1-ylacetonitrile (55.0 mg, 0.279 mmol) and Raney cobalt (500 mg) were suspended in 2M ammonia/methanol solution (10 mL), and the suspension was stirred at room temperature for 3 hr under a hydrogen atmosphere. The catalyst was filtered through celite, and the filtrate was concentrated under reduced pressure to give the title compound (55.5 mg, yield 99%).
WORKUP
后处理
- filtrationThe catalyst was filtered through celite
- concentrationthe filtrate was concentrated under reduced pressure