HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(methylsulfonyl)-2-[(1E)-prop-1-en-1-yl]aniline → 5-(Methylsulfonyl)-2-propylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(methylsulfonyl)-2-[(1E)-prop-1-en-1-yl]aniline | HCID 58522013 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5-(Methylsulfonyl)-2-propylaniline | HCID 58522006 | — |
Reaction Steps
A mixture of 5-(methylsulfonyl)-2-[(1E)-prop-1-en-1-yl]aniline (Intermediate 60; 1.50 g; 6.84 mmol) and 10% Pd/C (196 mg) in MeOH (39 ml) was placed in a PARR reactor and treated with a pressure of 20 atm of hydrogen for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-a332f15c61344e31811bb892ece5d3f9 |
| Source note | uspto-grants-2012_09 |