HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 58522027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 56594115 | HCID 56594115 | — |
| Reactant | HCID 58521909 | HCID 58521909 | — |
| Product | HCID 58522027 | HCID 58522027 | — |
Reaction Steps
Following the general method as outlined in Intermediate 253, starting from 4-bromo-2-(isopropylsulfonyl)benzoic acid (Intermediate 242) and dimethylamine, the title compound was obtained as a pink solid after purification by flash column chromatography (silica), eluting with cyclohexane containing increasing amounts of EtOAc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-79a4435221c54fa48ffca39cf966f486 |
| Source note | uspto-grants-2012_09 |