HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-chloro-4-ethynyl- → HCID 46865760, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-chloro-4-ethynyl- | HCID 70118 | — |
| Reactant | tert-Butyl (2-bromo-4-chlorophenoxy)acetate | HCID 49766393 | — |
| Product | HCID 46865760 | HCID 46865760 | — |
Reaction Steps
Following the general method as outlined in Example 1, starting from tert-butyl(2-bromo-4-chlorophenoxy)acetate (Intermediate 1) and 4-chlorophenylacetylene (Apollo), the title compound was obtained as a beige solid after purification by preparative HPLC
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-41a7c15dc3ff47a5b2f252a6f2119ec5 |
| Source note | uspto-grants-2012_09 |