HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-3-ethynylbenzene → HCID 46865762, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-3-ethynylbenzene | HCID 123086 | — |
| Reactant | tert-Butyl (2-bromo-4-chlorophenoxy)acetate | HCID 49766393 | — |
| Product | HCID 46865762 | HCID 46865762 | — |
Reaction Steps
Following the general method as outlined in Example 1, starting from tert-butyl(2-bromo-4-chlorophenoxy)acetate (Intermediate 1) and 3-chloro-1-ethynylbenzene (Aldrich), the title compound was obtained as a brown solid after purification by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-ec11ec7c15c94e9f87a23dee48a6f2fa |
| Source note | uspto-grants-2012_09 |