HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromopyridine → HCID 56594384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Reactant | Tert-butyl(4-chloro-2-ethynylphenoxy)acetate | HCID 56594381 | — |
| Product | HCID 56594384 | HCID 56594384 | — |
Reaction Steps
Following the general method as outlined in Example 10, starting from tert-butyl(4-chloro-2-ethynylphenoxy)acetate (Intermediate 3) and 3-bromopyridine (Fluka), the title compound was obtained as an off-white solid after purification by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-e586d318626040668337f48cc8d8004d |
| Source note | uspto-grants-2012_09 |